Performance Specifications of Asuragen Labeling method combined with Affymetrix GeneChip® miRNA Array*

Performance specifications of the miRNA Profiling Service using the Affymetrix GeneChip miRNA Array reflect the robustness of the Affymetrix platform and the superiority of Asuragen's labeling method.

Performance Specifications
Metric Asuragen's method
Recommended Input 100 ng total RNA for tissues (no fractionation required); 200 ng for FFPE and cell lines
LOD1 < 1 amol
Dynamic Range1 > 2.5 logs
Reproducibility (R2)2 0.97 (median CV < 4%)
Dose-Response Linearity (R2)1 0.99
Relative Accuracy1,3 1.02 ± 0.26
Specificity4 < 15% cross-hyb signal (average) from highly related, similar sequences with > 1 nt sequence differences
Sample QC Incoming sample QC by Spectrophotometer, and TaqMan RT-qPCR.
If, for any reason, a qualified sample does not pass our process control specifications, we will re-run the sample at no additional charge.

Footnotes:

1... Limit of Detection (LOD, Dynamic Range, Dose-Response Linearity, and Relative Accuracy are all based on latin-square spike-in study in a complex background of placenta total RNA processed according to the Affymetrix GeneChip Array Service protocols using the Asuragen labeling method.

2... Reproducibility reflects linear R2 values between full-process technical replicates.

3... Relative accuracy describes the degree to which the system responds to linear changes in the concentration of spike-in controls. The dose response slope measures the accuracy of reported fold-change relative to the known fold-change of a serial dilution series of miRNA spikes. A slope of 1.0 indicates perfect relative accuracy; slopes of approximately 0.8 are typical of microarray-based platforms as they are known to compress data.

4... Specificity of Affymetrix GeneChip Array is based on performance assessment on let-7 family members.

Linear Dynamic Range

Two process replicates are demonstrated here, illustrating the range of spikes used in the Latin-square design (1 amol to 316 amol). Note that the range defined by the spikes brackets the biologically relevant range of the placenta total RNA.

Linear Dynamic Range

Outstanding correlation with RT-qPCR and other commercially available platforms, even from fixed (FFPE) tissues

Eight FFPE blocks corresponding to four samples of two different tissue types (A and B) from eight different patients were purchased from Proteogenex Inc (Culver City, CA). All paraffin blocks were less than two years old. Total RNA was extracted from each of these blocks by Asuragen’s FFPE RNA isolation services team. 100 ng of total RNA isolated from each FFPE sample was analyzed using the Affymetrix GeneChip miRNA array and Asuragen labeling method; 200 ng of total RNA was analyzed using the Agilent V2 miRNA Array and 500 ng of total RNA was analyzed with the Asuragen miRLink Service.

A series of qRT-PCR reactions were performed using TaqMan microRNA assays# specific for 6 different miRNAs following manufacturer’s instructions and using an input of 15ng total RNA per reaction. Real-time reactions were run on the 7900HT fast realtime PCR system# and initial analysis of data was done using the SDS 2.3 software included.

The following figures demonstrate the remarkable correlation between the RT-qPCR data and the data obtained from different array-based platforms with high statistical significance (p-values as shown). These p-values demonstrate the overall reproducibility of the Asuragen profiling service using the Affymetrix GeneChip miRNA array and Asuragen labeling method.

plarform comparison Affymetrix GeneChip

In all figures, the array data shown are VSN normalized values and the TaqMan data are ΔCTs.

Interested in Asuragen's other miRNA services? [Click here]

#...(Applied Biosystems, Foster City, CA, USA)
*...For Research Use Only. Not for use in diagnostic procedures.

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